This work is focused on the development of a clean-up method with the AZURA® GPC Cleanup system to purify soil sample extracts before analysis. It was found that GPC cleanup is very useful to remove interferences from extracted soil samples before GC-MS/MS determination of semi-volatile organic compounds, like Polycyclic Aromatic Hydrocarbons. Moreover, the described method enables to perform an automated clean-up procedure and hence to purify many samples efficiently.
Chromatogram of a diluted calibration mixture solution 1) Corn oil (5 mg/mL), 2) Phthalic acid, bis-2-ethylhexyl ester (1 g/L), 3) Methoxychlor (0.2 g/L), 4) Perylene (0.02 g/L), 5) Sulfur (0.08 g/L)
GC-MS/MS chromatogram of purified soil sample: determination of PAHs
GC-MS/MS chromatogram of purified soil sample: determination of PAHs
| Methode | GC/MS |
|---|
| Modus | GPC |
|---|---|
| Substanzen | Polycyclic aroamtic hydrocarbons |
| Schlüsselwörter | GPC Cleanup, GPC, SPE, PAH, polycyclic aroamtic hydrocarbons, UNI EN 15527: 2008 |
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